Oxidation and Reduction of Ir(100) Studied by High-Energy Surface X-ray Diffraction
The oxidation and reduction of an Ir(100) surface using 2.5, 5, and 10 mbar O2partial pressure and a sample temperature of 775 K have been studied by using high-energy surface X-ray diffraction (HESXRD) which allowed to record large volumes of reciprocal space in short time periods. The complex 3D diffraction patterns could be disentangled in a stepwise procedure. For the 2.5 mbar experiment the m